Error 10cm3 Graduated Pipette
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50cm3 Measuring Cylinder Uncertainty
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Percentage Error Of 25cm3 Pipette
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developed between September 2011 and April 2012, and new content will be added
10cm3 Pipette
on a day-to-day basis during that period. Please send any comments/suggestions to 10cm3 measuring cylinder graham.currell@uwe.ac.uk Study Text: "Essential Mathematics and Statistics for Science", 2nd ed, G Currell and A A Dowman
100 Cm3 Measuring Cylinder Uncertainty
(Wiley-Blackwell) QVA (questions and video answers) Tutorials: Combining uncertainties / propagation of errorsStudy Text: Section 8.3.3 (p226) Errors and uncertainties in concentrations and dilutions (video feedback in preparation) http://www.thestudentroom.co.uk/showthread.php?t=363038 Study Text: Section 8.3.3 (p226) Combining and propagating random errors/uncertainties Assuming random uncertainties where: ua and ub are the absolute uncertainties in variables, a and b. Rua and Rub are the relative percentage uncertainties in variables, a and b. To convert between absolute and relative percentage uncertainties: Rua = 100 × ua / a and ua = http://calcscience.uwe.ac.uk/combinations-of-errors.aspx a × Rua / 100 etc To calculate combined uncertainties use absolute or relative uncertainties depending on the combination of variables which give a final value x: If • x = a + b or x = a - b :- thenuse ux = √{(ua)2 + (ub)2} • x = a×b or x = a/b :- then use Rux = √{(Rua)2 + (Rub)2} • x = k×a (where k is a constant):- then use Rux = Rua or ux = k×ua • x = an (where n is a constant) :- then use Rux = n×(Rua) Note that it is possible to use the simple (not percentage) relative uncertainties (i.e. without introducing the ‘100’ into the calculations), but it is necessary to be consistent throughout the calculation. We use percentage uncertainty here because many scientists are more familiar with expressing relative uncertainty as a percentage. See Study Text: Section 8.3.3 Absolute and relative uncertainty The uncertainty of ±0.03 cm3 in a 10 cm3 class A graduated pipette would be c
point End point indicators End point detection Equivalence point calculation Titration curve calculation Titration calculation Back titration Sample & titrant volume Volumetric glassware Volumetric glass cleaning Glassware calibration Standard substances Sources of errors Need more http://www.titrations.info/pipette-burette info? Dean's Analytical Chemistry Handbook by Pradyot Patnaik Complete list of books Titration » Burette, pipette, flask - volumetric glassware During titration experiments you will be using several types of volumetric glass. They all are designed to help measure volume of a liquid. Some types of the volumetric glass can be used only to measure predefined volume of solution. These are volumetric flasks and single volume measuring cylinder pipettes. They are characterised by a a high accuracy and repeatability of measurements. Flasks are designed to contain (TC, sometimes marked as IN) known volume of the solution, while pipettes are generally designed to deliver (TD, sometimes marked as EX) known volume (although in some rare cases they can be designed to contain). This is an important distinction - when you empty pipette you deliver exactly percentage error of required volume and you dont have to worry about the solution that is left on the pipette walls and in pipette tip. At the same time you will never know how much solution was in the pipette. On the contrary, volumetric flask is known to contain required volume, but if you will pour the solution to some other flask you will never know how much of the solution was transferred. Both kinds of glass were designed this way as they serve different purposes. Volumetric flask is used to dilute original sample to known volume, so it is paramount that it contains exact volume. Pipette is used to transfer the solution, so it is important that it delivers known volume. Note, that volumetric pipettes are designed in such a way that after a fluid is dispensed, a small drop of liquid will remain in the tip. In general you should not blow this drop out. The correct volume will be dispensed from the pipette if the side of the tip is touched to the inside wall of the flask (or beaker). Third kind of precise volumetric glass is burette. Burette is used to add titrant to t
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