20 Ml Pipette Error
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point End point indicators End point detection Equivalence point calculation Titration curve calculation Titration calculation Back titration Sample & titrant volume Volumetric glassware Volumetric glass cleaning Glassware calibration Standard substances Sources of errors 25 ml pipette uncertainty Need more info? Measurement Uncertainty in Chemical Analysis by Paul De Bievre
10 Ml Pipette Uncertainty
(Editor) Complete list of books Titration » Burette, pipette, flask - volumetric glassware During titration experiments you will be 5 ml pipette uncertainty using several types of volumetric glass. They all are designed to help measure volume of a liquid. Some types of the volumetric glass can be used only to measure predefined volume of uncertainty of 50 ml pipette solution. These are volumetric flasks and single volume pipettes. They are characterised by a a high accuracy and repeatability of measurements. Flasks are designed to contain (TC, sometimes marked as IN) known volume of the solution, while pipettes are generally designed to deliver (TD, sometimes marked as EX) known volume (although in some rare cases they can be designed to contain). This is an
1 Ml Pipette
important distinction - when you empty pipette you deliver exactly required volume and you dont have to worry about the solution that is left on the pipette walls and in pipette tip. At the same time you will never know how much solution was in the pipette. On the contrary, volumetric flask is known to contain required volume, but if you will pour the solution to some other flask you will never know how much of the solution was transferred. Both kinds of glass were designed this way as they serve different purposes. Volumetric flask is used to dilute original sample to known volume, so it is paramount that it contains exact volume. Pipette is used to transfer the solution, so it is important that it delivers known volume. Note, that volumetric pipettes are designed in such a way that after a fluid is dispensed, a small drop of liquid will remain in the tip. In general you should not blow this drop out. The correct volume will be dispensed from the pipette if the side of the tip is touched to the inside wall of the flask (o
ChemLab Home Before Lab This week, plan to spend extra time on prelab preparation. Make your prelab procedure outline or flowchart clear and 1 ml pipette uncertainty complete, to cover all possible contingencies. You should meet with your 20 ml volumetric pipette partner to plan your strategy before coming to lab. Both partners should contribute to the procedure
Burette Uncertainty
planning. Since you will plan your procedure together, the content of your prelab procedures may be very similar. Include a high level of detail in your sample calculations http://www.titrations.info/pipette-burette or analysis outline or flowchart. The better prepared you are before lab, the more smoothly your experiments will go. Be sure to complete your prelab problems. In Lab Record your observations and your data, with citation of your lab partner's notebook, if necessary. Clear and complete titration data will help you to analyze your results. For https://www.dartmouth.edu/~chemlab/chem3-5/acid2/full_text/write-up.html the acid and base solutions, remember that you must determine the concentration to within 3 significant figures. If time allows, repeat this determination to assess your reproducibility. Uncertainty Analysis For this week's experiment, you will have qualitative results, the identity of your solutions, and quantitative results, the concentrations of acid or base solutions. For the concentration determinations, you will do an uncertainty analysis to evaluate the precision of your results. Since your have a small number of results, a statistical analysis is not appropriate. This week, you will use significant figures as an approximate way of estimating the uncertainty in the solution concentrations that you determine. While in the lab, record the uncertainty in your volume measurements, both for buret readings and for pipets you might use for delivery of a sample for titration. Use these uncertainty values to determine the correct number of significant figures for each value your record. For example, a 20 mL volumetric pipet has an uncertainty of ±0.06 mL. Since
Engineering Medicine Agriculture Photosciences Humanities Periodic Table of the Elements Reference Tables Physical Constants Units and Conversions Organic Chemistry Glossary Search site Search Search Go http://chem.libretexts.org/Textbook_Maps/Analytical_Chemistry_Textbook_Maps/Map%3A_Analytical_Chemistry_2.0_(Harvey)/04_Evaluating_Analytical_Data/4.3%3A_Propagation_of_Uncertainty back to previous article Username Password Sign in Sign in Sign in Registration Forgot password Expand/collapse global hierarchy Home Textbook Maps Analytical Chemistry Textbook Maps Map: Analytical Chemistry 2.0 (Harvey) 4: Evaluating Analytical Data Expand/collapse global location 4.3: Propagation of Uncertainty Last updated 10:52, 25 May 2016 Save as PDF Share Share Share Tweet Share 4.3.1 A Few Symbols4.3.2 ml pipette Uncertainty When Adding or Subtracting4.3.3 Uncertainty When Multiplying or Dividing4.3.4 Uncertainty for Mixed Operations4.3.5 Uncertainty for Other Mathematical Functions4.3.6 Is Calculating Uncertainty Actually Useful?Contributors Suppose you dispense 20 mL of a reagent using the Class A 10-mL pipet whose calibration information is given in Table 4.9. If the volume and uncertainty for one use of the pipet is 9.992 ± ml pipette uncertainty 0.006 mL, what is the volume and uncertainty when we use the pipet twice? As a first guess, we might simply add together the volume and the maximum uncertainty for each delivery; thus \[\mathrm{(9.992\: mL + 9.992\: mL) ± (0.006\: mL + 0.006\: mL) = 19.984 ± 0.012\: mL}\] It is easy to appreciate that combining uncertainties in this way overestimates the total uncertainty. Adding the uncertainty for the first delivery to that of the second delivery assumes that with each use the indeterminate error is in the same direction and is as large as possible. At the other extreme, we might assume that the uncertainty for one delivery is positive and the other is negative. If we subtract the maximum uncertainties for each delivery, \[\mathrm{(9.992\: mL + 9.992\: mL) ± (0.006\: mL - 0.006\: mL) = 19.984 ± 0.000\: mL}\] we clearly underestimate the total uncertainty. So what is the total uncertainty? From the previous discussion we know that the total uncertainty is greater than ±0.000 mL and less than ±0.012 mL. To estimate the cumulati
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