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3 Ml Pipette Error

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deliver a volume known to a few hundredths of a milliliter, or about 0.01 mL. One can then report quantities greater than 10 mL to four significant figures. Glassware designed for this level of accuracy and precision is expensive, and requires some care 3ml pipette and skill to give best results. Four main types of volumetric glassware are common: the graduated

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cylinder, the volumetric flask, the buret and the pipet. These have specific uses and will be discussed individually. There are some points that are

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common to all types, however. These involve cleanliness and how to read volumes accurately. Cleanliness is essential to good results. Chemically clean glass supports a uniform film of water, with no hanging droplets visible. Rinse your glassware thoroughly with deionized http://www.sigmaaldrich.com/catalog/product/aldrich/cls71033?lang=en&region=US water when you are finished with it. If you are suspicious at all, wash it before you use it as well. With some types of glassware, one "conditions" the apparatus by rinsing with a few small portions of the solution one will be measuring prior to conducting the actual work. This prevents water droplets from diluting one's solution, and changing the concentration. More detail on how to do this will be given in the discussion of the individual pieces http://www.webassign.net/question_assets/tccgenchem2l1/glassware/manual.html of glassware. All volumetric glassware is calibrated with markings used to determine a specific volume of liquid to varying degrees of accuracy. To read this volume exactly, the bottom of the curved surface of the liquid, the meniscus, should be located at the scribed line for the desired volume. It is often easier to see the meniscus if you put a white paper or card behind the apparatus. If your eye is above or below the level of the meniscus, your readings will be inaccurate due to the phenomenon of parallax. View the meniscus at a level perpendicular to your eye to avoid this as a source of error. TC Versus TD Some volumetric glassware bears the label "TC 20°C" which stands for "to contain at 20°C." This means that at 20°C, that flask will have precisely the volume listed inside it. If you were to pour out the liquid, you would need to get every drop out of it to have that volume. Alternatively, some volumetric glassware bears the label "TD 20°C" which stands for "to deliver at 20°C." This means that at 20°C, precisely the volume listed will leave it when the contents are allowed to drain out of the vessel. It is not necessary to get every last drop and, in fact, it is inaccurate to blow the last bit out of a volumetric pipet. Graduated Cylinders Most students are familiar with graduated cy

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